网页Jun 22, 2019 · 1. Pour and dry the liquid in the chromatographic sample bottle. 2. 2. Pour dry after this as the alcohol enters the 1.5mL vial easily and is intersoluble with most organic solvents. 3. Pour in water and wash with ultrasonic twice. 4. Pour the liquid in the bottle and bake at 110 ° c for 1~2 hours.